Solubility - preferred solvent:
DMSO
Solubility - concentration:
20 mM
NMR:
1H NMR (400 MHz, DMSO-d6) δ 11.54 (s, 1 H), 8.65 (t, J=4.80 Hz, 1 H), 8.40 (s, 1 H), 8.24 (s, 1 H), 8.21 (d, J=5.30 Hz, 1 H), 7.86 (s, 1 H), 7.21 (s, 1 H), 7.14 (d, J=5.31 Hz, 1 H), 5.91 (s, 1 H), 5.21 (dt, J=13.14, 6.57 Hz, 1 H), 4.42 (d, J=4.80 Hz, 2 H), 3.56 - 3.63 (m, 4 H), 2.53 - 2.56 (m, 2 H), 2.44 (t, J=4.93 Hz, 4 H), 2.24 (s, 3 H), 2.13 (s, 3 H), 1.52 - 1.61 (m, 2 H), 1.52 (s, 3 H), 1.50 (s, 3 H), 0.89 (t, J=7.33 Hz, 3 H);
13C NMR (100 MHz, DMSO-d6) δ 165.5, 163.4, 159.8, 153.6, 148.7, 148.1, 142.9, 139.3, 135.7, 132.7, 128.0, 121.4, 121.3, 119.2, 111.9, 110.5, 106.3, 104.9, 55.5 (2C), 49.1, 45.8, 44.7 (2C), 34.8, 34.2, 22.9, 22.2 (2C), 18.3, 13.9;
Chemical Probes Portal GSK343.pdf
